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 · Mechanical milling is a promising route for production of submicron and nano sized silicon powders, but it is challenging to predict and control the product properties. In this study a metallurgical grade silicon quality was milled in a planetary ball mill and the properties of the powder were investigated as a function of grinding time, grinding bead size (20 mm, 2 mm, 0.25 mm) and …

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Jun 16, 2011 Fig. 1, Fig. 2 show the X-ray diffraction patterns of the ZnSe mixtures milled for various times t M in both types of mills.As indicated in Fig. 1, zinc selenide ZnSe, JCPDS 15-0105 is formed after 18 min of milling in the laboratory ball mill. On the other hand, this mechanosynthesized product is formed already after t M 15 min in the industrial vibratory mill.

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